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Por qué un analizado directo ed mercurio es la opción preferida para la determinación de mercurio en muestras medioambientales?

dma environmental big

Existen varios métodos para la determinación de mercurio en aguas y suelos, pero la mayoría requieren elaborados procedimientos para la preparación de las muestras y por consiguiente son tediosos y caros.
El análisis directo de mercurio, descrito en la norma EPA 7473, es una alternativa a los métodos anteriores que ha sido empleada satisfactoriamente en la determinación de mercurio en muestras medioambientales.
Esta técnica no requiere una preparación de las muestras y ofrece resultados en menos de 6 minutos, haciéndola significativamente más rápida que los métodos tradicionales por vía húmeda.

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Digestión de Crudo Pesado en cámara de reacción única (SRC)

JAAS

El análisis elemental de crudo pesado es importante por múltiples razones como por ejemplo, determinar la región de origen, la madurez, la migración, el tipo, etc. Y la identificación de factores que pueden afectar al proceso de refino. Este análisis presenta numerosas dificultades, la mayoría relacionadas con el proceso de preparación de la muestra, debido a la complejidad de la matriz.
La digestión mediante microondas ha servido para superar parte de esas dificultades, sin embargo, los sistemas tradicionales de rotores de vaso cerrado, siguen presentando algunos problemas relacionados con los límites de cuantificación, el carbono orgánico residual y la acidez residual.
El artículo recientemente publicado "Rare earth element determination in heavy crude oil by USN-ICP-MS after digestion using a microwave-assisted single reaction chamber", Druzian et al, J. Anal. At. Spectrom., 2016, 31, 1185, compara la cantidad máxima de muestra de petróleo crudo que se puede digerir y la calidad de la digestión, con dos equipos de microondas: UltraWAVE de Milestone (UW) y Multiwave 3000 de Anton Paar.
Este trabajo propone un método para la determinación de elementos de tierras raras, mediante espectrometría de masas con plasma de acoplamiento inductivo, tras una digestión ácida por microondas utilizando nuestro UltraWAVE.
Atendiendo a las conclusiones, este es el primer método capaz de digerir 1 gramo de petróleo crudo mediante digestión ácida en vaso cerrado, permitiendo la determinación de aquellos elementos presentes en muy baja concentración. La eficiencia de la digestión es mayor usando el UltraWAVE, al proporcionar unos contenidos residuales de carbono orgánico y acidez mucho menores, parámetros importantes para evitar interferencias durante la determinación de elementos de tierras raras por ICP-MS. El UltraWAVE combina un rendimiento y una seguridad excelentes, además de una productividad relativamente alta, ya que podría realizar la digestión simultánea de hasta cinco muestras en 40 minutos.
Finalmente, tanto los límites de cuantificación como la acidez residual, son menores que los obtenidos usando el Multiwave 3000 de Anton Paar.
Puede leer el artículo completo aquí…http://pubs.rsc.org/en/content/articlelanding/2016/ja/c6ja00050a#!divAbstract

 


Complimentary, live webinar: Microwave technology applied to inorganic synthesis

Complimentary, live webinar
Microwave technology applied to inorganic synthesis: what is going to change?

vip2Inorganic synthesis is an important branch of the chemical synthesis with the aim of the production of new materials with new functions for new applications.

Changing the conventional methodologies of inorganic synthesis to more environmental-friendly and cost effective methods has opened up new avenues to achieve an enhanced and novel sustainable chemistry, thus contributing to the preservation of the natural environment. These routes, such as the microwave assisted hydrothermal synthesis provide the use of microwaves combined with the efficiency of the hydrothermal method. This facilitate the engineering of a wide variety of high-quality materials such as nano-sized rare earth doped ceria with fluorite structure for SOFC electrolyte applications, BiFeO3 perovskite with multiferroic properties and H2V3O8 with one-dimensional (1D) nanostructure for lithium battery technology.

During this webinar, we will go through the complete and up-to-date possibilities offered by the combination of two rapid and “green chemistry” synthesis techniques: hydrothermal synthesis and microwave synthesis. The goal is to minimize heat exposure and reaction times for chemical synthesis. Moreover, the particle sizes and shapes of the product can be fine tuned by the synthesis parameters.

Take part in our complimentary, live webinar!

You’ll interact with the experts who are breaking ground in this field of research: Emilio Miguélez Morán, professor at University of Madrid and Diego Carnaroglio, PhD, synthesis specialist at Milestone Srl.

You’ll learn about the newest tools and technologies while gathering valuable tips and troubleshooting strategies for the applications most relevant to your processes.

VERLO AHORA

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PRESENTERS
 
Diego Carnaroglio, PhD
Synthesis and Extraction Application Specialist
at Milestone
 
In 2011 he received the Degree in Chemistry at the University of Turin and in 2014 he received the Ph.D. in Pharmaceutical and Biomolecular Sciences at the same university under the guidance of Prof. Giancarlo Cravotto with a thesis titled “Key enabling technologies for green, highly competitive chemical processes”. His research activity is documented by 20 scientific papers and 1 book chapter, 11 posters and 10 oral communications at international conferences. His collaboration with the University of Turin is still active, in order to developed new sustainable and green microwave processes.

 
Emilio Morán Miguélez, Prof.
Universidad Complutense
of Madrid
 
Full professor of Chemistry at the Universidad Complutense in Madrid and Head of Department of Inorganic Chemistry. Prof. Morán is an expert in the microwave assisted inorganic synthesis and solid state synthesis, “Fast and Soft Chemistry”. His efforts are in the synthesis of material for technological application such as superconductors, magnetic materials and solid electrolites.
He is the evaluation expert for ANECA, ACAP, ACSUG, AVAP, ANEP quality agencies and his research activity is documented by more than 200 scientific papers and several plenary contributions to international conferences.
 

Volver a ver: Detección de metales en alimentos?

Microwave digestion of food samples

WEBINAR: detección de metales en muestras de alimentos

Análisis de bajo nivel de matrices de alimentos ha puesto una demanda para los fabricantes, laboratorios de análisis y proveedores de instrumentación en todo el mundo.
Regulaciones más estrictas, una mejor instrumentación analítica, y la mejora técnicas de la preparación de muestras (preanalíticos) se han centrado para simplificar y estandarizar estos análisis.
Este seminario proporcionará el fondo de las tecnologías utilizadas para la digestión de microondas y sus ventajas hacia estos temas relacionados con la alimentación. Los últimos acontecimientos en relación con configuraciones de instrumentos disponibles, los límites de detección, preparación de muestras, y más se discutirán.

VERLO AHORA

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Nuevos horizontes en síntesis química asistida por microondas

flexi-b

WEBINAR: Nuevos horizontes en síntesis química asistida por microondas: flexibilidad y alta presión

10 noviembre, 2015

How can this benefit your research?
… Imagine que es capaz de realizar reacciones complejas con una sola herramienta, superando las limitaciones de otros sistemas de sìntesis microondas. Esto es posble con flexiWAVE , una única plataforma microondas que permite a los usuarios llevar a cabo sintesis convencionales y de alta presión , así como reacciones en fase sólida en un solo paso, obteniendo productos de alta pureza en menor cantidad de tiempo.
… Imagine being able to better control reactions to get faster results and screen multiple reactions simultaneously. synthWAVE enables to vary the solvent or catalyst or even how many different reactions can be run in a single reaction vessel - simultaneously.

WATCH OUR WEBCAST HERE

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Webinar: Soluciones innovadoras para aumento de la productividad en los laboratorios comerciales

contractlabs

WEBINAR: Novel solutions for increasing productivity in commercial contract labs?

Without question, the ultimate goal of your lab should be to find a flexible, easy-to-use sample preparation solution for preparing any element, in a variety of matrices, over a wide concentration range.
Standardizing multi-element sample preparation to include little to no method development, the capability of processing mixed sample batches and simultaneous detection techniques offers a cost effective solution to increase laboratory productivity.
Milestone provide complete solutions for today’s contract laboratory needs.
This interactive webinar will highlight how you can advance your contract lab’s capabilities with novel sample prep solutions.

WATCH THE RECORDING NOW: CLICK HERE

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Capacitación y seminarios

seminarsMilestone organiza sistemáticamente cursos interno de capacitación sobre diferentes temas de aplicación.

La invitación está abierta a todos los químicos que deseen adquirir más conocimientos sobre la preparación de muestras, la determinación de mercurio o síntesis.

Podrá consultar a nuestros especialistas en aplicaciones de forma individual para resolver sus problemas.

Contáctenos para suscribirse!

 


¡Prepárese para la implementación de los capítulos de USP 232 y 233!

Microwave digestion of pharma samples

WEBINAR: Practical Guidance on Sample Preparation of Elemental Impurities in Pharmaceutical Samples

Impurities in pharmaceutical products are of great concern not only due to the inherent toxicity of certain contaminats, but also due to the adverse effect that contaminats may have on drug stability and shelf-life.
The current USP “heavy metals limit test” is due to be replaced with new USP 232 General Chapters USP (Limits) and USP 233 (Procedures revision).
This webinar will provide the background on the development of the new General Chapters and explain how closed vessel microwave digestion can address the requirements of the proposed new methods. The latest developments regarding detection limits, implementation dates, and more will be discussed. In addition, this webinar will take an in depth look at a new approach that has revolutionized how labs operate removing all the barriers of traditional techniques while offering high ROI for labs needing high throughput and mixed batch runs.

VIEW THE RECORDING NOW

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